| Rigaku R-AXIS RAPID diffractometer | 1211 reflections with F2 > 2.0σ(F2) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.079 |
| ω scans | θmax = 68.2°, θmin = 4.7° |
| Absorption correction: multi-scan (ABSCOR; Rigaku, 1995) | h = −6→6 |
| Tmin = 0.729, Tmax = 0.878 | k = −8→8 |
| 6710 measured reflections | l = −12→12 |
| 1329 independent reflections |
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