Bruker SMART APEX CCD diffractometer | 3808 independent reflections |
Radiation source: fine-focus sealed tube | 3114 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.079 |
ω–scans | θmax = 25.4°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −45→45 |
Tmin = 0.349, Tmax = 0.745 | k = −7→7 |
16925 measured reflections | l = −20→20 |