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. 2015 Sep 26;71(Pt 10):1230–1235. doi: 10.1107/S2056989015017181
Bruker SMART APEX CCD diffractometer 3808 independent reflections
Radiation source: fine-focus sealed tube 3114 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.079
ω–scans θmax = 25.4°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2012) h = −45→45
Tmin = 0.349, Tmax = 0.745 k = −7→7
16925 measured reflections l = −20→20