Bruker SMART APEX CCD diffractometer | 3961 independent reflections |
Radiation source: fine-focus sealed tube | 2941 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.079 |
Detector resolution: 8.333 pixels mm-1 | θmax = 25.4°, θmin = 1.7° |
ω–scans | h = −10→10 |
Absorption correction: multi-scan (TWINABS; Bruker, 2012) | k = 0→28 |
Tmin = 0.273, Tmax = 0.429 | l = 0→12 |
3961 measured reflections |