| Siemens SMART CCD area-detector diffractometer | 11921 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.040 |
| phi and ω scans | θmax = 40.2°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −19→18 |
| Tmin = 0.133, Tmax = 0.478 | k = −25→26 |
| 93039 measured reflections | l = −28→27 |
| 14497 independent reflections |
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