Skip to main content
. 2015 Sep 26;71(Pt 10):1212–1215. doi: 10.1107/S2056989015017582
O1—C1 1.412 (2) C13—C16 1.498 (3)
O1—C4 1.442 (2) C13—C15 1.519 (3)
C1—O12 1.404 (2) C15—H15A 0.9600
C1—C2 1.526 (3) C15—H15B 0.9600
C1—H1 0.9800 C15—H15C 0.9600
C2—O14 1.433 (2) C16—H16A 0.9600
C2—C3 1.519 (3) C16—H16B 0.9600
C2—H2 0.9800 C16—H16C 0.9600
C3—C3' 1.519 (3) C3'—N4' 1.457 (3)
C3—C4 1.535 (3) C3'—H3'1 0.9700
C3—H3 0.9800 C3'—H3'2 0.9700
C4—C5 1.520 (3) N4'—C5' 1.346 (3)
C4—H4 0.9800 N4'—H4' 0.80 (3)
C5—O9 1.427 (2) C5'—O6' 1.209 (3)
C5—C6 1.527 (3) C5'—O7' 1.355 (3)
C5—H5 0.9800 O7'—C8' 1.450 (3)
C6—O7 1.424 (3) C8'—C1'' 1.502 (3)
C6—H6A 0.9700 C8'—H8'1 0.9700
C6—H6B 0.9700 C8'—H8'2 0.9700
O7—C8 1.424 (2) C1''—C2'' 1.384 (4)
C8—O9 1.443 (2) C1''—C6'' 1.387 (4)
C8—C10 1.501 (3) C2''—C3'' 1.376 (4)
C8—C11 1.519 (3) C2''—H2'' 0.9300
C10—H10A 0.9600 C3''—C4'' 1.382 (4)
C10—H10B 0.9600 C3''—H3'' 0.9300
C10—H10C 0.9600 C4''—C5'' 1.367 (5)
C11—H11A 0.9600 C4''—H4'' 0.9300
C11—H11B 0.9600 C5''—C6'' 1.387 (4)
C11—H11C 0.9600 C5''—H5'' 0.9300
O12—C13 1.424 (3) C6''—H6'' 0.9300
C13—O14 1.435 (3)
C1—O1—C4 110.30 (15) C1—O12—C13 110.36 (16)
O12—C1—O1 111.76 (17) O12—C13—O14 105.28 (15)
O12—C1—C2 105.29 (17) O12—C13—C16 108.82 (19)
O1—C1—C2 106.75 (16) O14—C13—C16 109.43 (18)
O12—C1—H1 110.9 O12—C13—C15 109.1 (2)
O1—C1—H1 110.9 O14—C13—C15 110.69 (19)
C2—C1—H1 110.9 C16—C13—C15 113.2 (2)
O14—C2—C3 110.74 (16) C2—O14—C13 107.18 (15)
O14—C2—C1 102.96 (16) C13—C15—H15A 109.5
C3—C2—C1 103.87 (16) C13—C15—H15B 109.5
O14—C2—H2 112.8 H15A—C15—H15B 109.5
C3—C2—H2 112.8 C13—C15—H15C 109.5
C1—C2—H2 112.8 H15A—C15—H15C 109.5
C2—C3—C3' 115.04 (17) H15B—C15—H15C 109.5
C2—C3—C4 101.29 (16) C13—C16—H16A 109.5
C3'—C3—C4 116.30 (17) C13—C16—H16B 109.5
C2—C3—H3 107.9 H16A—C16—H16B 109.5
C3'—C3—H3 107.9 C13—C16—H16C 109.5
C4—C3—H3 107.9 H16A—C16—H16C 109.5
O1—C4—C5 106.73 (15) H16B—C16—H16C 109.5
O1—C4—C3 103.54 (15) N4'—C3'—C3 109.09 (17)
C5—C4—C3 117.26 (16) N4'—C3'—H3'1 109.9
O1—C4—H4 109.7 C3—C3'—H3'1 109.9
C5—C4—H4 109.7 N4'—C3'—H3'2 109.9
C3—C4—H4 109.7 C3—C3'—H3'2 109.9
O9—C5—C4 110.29 (16) H3'1—C3'—H3'2 108.3
O9—C5—C6 103.92 (14) C5'—N4'—C3' 121.7 (2)
C4—C5—C6 115.15 (17) C5'—N4'—H4' 116.9 (18)
O9—C5—H5 109.1 C3'—N4'—H4' 120.3 (18)
C4—C5—H5 109.1 O6'—C5'—N4' 125.9 (2)
C6—C5—H5 109.1 O6'—C5'—O7' 125.2 (2)
O7—C6—C5 103.79 (16) N4'—C5'—O7' 108.9 (2)
O7—C6—H6A 111.0 C5'—O7'—C8' 117.5 (2)
C5—C6—H6A 111.0 O7'—C8'—C1'' 106.1 (2)
O7—C6—H6B 111.0 O7'—C8'—H8'1 110.5
C5—C6—H6B 111.0 C1''—C8'—H8'1 110.5
H6A—C6—H6B 109.0 O7'—C8'—H8'2 110.5
C6—O7—C8 105.08 (16) C1''—C8'—H8'2 110.5
O7—C8—O9 104.38 (16) H8'1—C8'—H8'2 108.7
O7—C8—C10 108.31 (18) C2''—C1''—C6'' 118.9 (2)
O9—C8—C10 109.48 (17) C2''—C1''—C8' 120.8 (2)
O7—C8—C11 111.69 (17) C6''—C1''—C8' 120.2 (3)
O9—C8—C11 109.16 (17) C3''—C2''—C1'' 120.6 (3)
C10—C8—C11 113.42 (18) C3''—C2''—H2'' 119.7
C5—O9—C8 108.74 (14) C1''—C2''—H2'' 119.7
C8—C10—H10A 109.5 C2''—C3''—C4'' 120.4 (3)
C8—C10—H10B 109.5 C2''—C3''—H3'' 119.8
H10A—C10—H10B 109.5 C4''—C3''—H3'' 119.8
C8—C10—H10C 109.5 C5''—C4''—C3'' 119.4 (3)
H10A—C10—H10C 109.5 C5''—C4''—H4'' 120.3
H10B—C10—H10C 109.5 C3''—C4''—H4'' 120.3
C8—C11—H11A 109.5 C4''—C5''—C6'' 120.8 (3)
C8—C11—H11B 109.5 C4''—C5''—H5'' 119.6
H11A—C11—H11B 109.5 C6''—C5''—H5'' 119.6
C8—C11—H11C 109.5 C5''—C6''—C1'' 119.9 (3)
H11A—C11—H11C 109.5 C5''—C6''—H6'' 120.1
H11B—C11—H11C 109.5 C1''—C6''—H6'' 120.1
C4—O1—C1—O12 107.54 (18) C11—C8—O9—C5 −95.99 (19)
C4—O1—C1—C2 −7.1 (2) O1—C1—O12—C13 −111.56 (19)
O12—C1—C2—O14 −20.6 (2) C2—C1—O12—C13 4.0 (2)
O1—C1—C2—O14 98.33 (18) C1—O12—C13—O14 14.4 (2)
O12—C1—C2—C3 −136.12 (17) C1—O12—C13—C16 131.58 (19)
O1—C1—C2—C3 −17.2 (2) C1—O12—C13—C15 −104.5 (2)
O14—C2—C3—C3' 49.2 (2) C3—C2—O14—C13 140.31 (17)
C1—C2—C3—C3' 159.10 (16) C1—C2—O14—C13 29.82 (19)
O14—C2—C3—C4 −77.1 (2) O12—C13—O14—C2 −28.1 (2)
C1—C2—C3—C4 32.8 (2) C16—C13—O14—C2 −144.9 (2)
C1—O1—C4—C5 152.58 (16) C15—C13—O14—C2 89.6 (2)
C1—O1—C4—C3 28.2 (2) C2—C3—C3'—N4' 65.0 (2)
C2—C3—C4—O1 −37.23 (19) C4—C3—C3'—N4' −176.82 (16)
C3'—C3—C4—O1 −162.69 (16) C3—C3'—N4'—C5' −165.57 (19)
C2—C3—C4—C5 −154.43 (17) C3'—N4'—C5'—O6' 3.5 (4)
C3'—C3—C4—C5 80.1 (2) C3'—N4'—C5'—O7' −177.68 (18)
O1—C4—C5—O9 −67.04 (19) O6'—C5'—O7'—C8' 0.7 (3)
C3—C4—C5—O9 48.4 (2) N4'—C5'—O7'—C8' −178.11 (19)
O1—C4—C5—C6 175.77 (16) C5'—O7'—C8'—C1'' 153.0 (2)
C3—C4—C5—C6 −68.8 (2) O7'—C8'—C1''—C2'' 67.3 (3)
O9—C5—C6—O7 −20.8 (2) O7'—C8'—C1''—C6'' −109.6 (3)
C4—C5—C6—O7 99.97 (19) C6''—C1''—C2''—C3'' 0.9 (4)
C5—C6—O7—C8 35.75 (19) C8'—C1''—C2''—C3'' −176.1 (2)
C6—O7—C8—O9 −37.11 (19) C1''—C2''—C3''—C4'' −0.5 (4)
C6—O7—C8—C10 −153.69 (17) C2''—C3''—C4''—C5'' −0.3 (4)
C6—O7—C8—C11 80.7 (2) C3''—C4''—C5''—C6'' 0.7 (4)
C4—C5—O9—C8 −125.60 (16) C4''—C5''—C6''—C1'' −0.3 (4)
C6—C5—O9—C8 −1.7 (2) C2''—C1''—C6''—C5'' −0.5 (4)
O7—C8—O9—C5 23.5 (2) C8'—C1''—C6''—C5'' 176.5 (2)
C10—C8—O9—C5 139.31 (17)