| Bruker APEXII CCD area detector diffractometer | 7103 independent reflections |
| Radiation source: Bruker TXS fine-focus rotating anode | 6001 reflections with I > 2σ(I) |
| Bruker Helios multilayer confocal mirror monochromator | Rint = 0.038 |
| Detector resolution: 8.333 pixels mm-1 | θmax = 27.5°, θmin = 1.6° |
| phi and ω scans | h = −22→22 |
| Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −23→23 |
| Tmin = 0.48, Tmax = 0.80 | l = −25→25 |
| 35025 measured reflections |
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