Table 3. Experimental details.
Crystal data | |
Chemical formula | [Pt(C11H7BrN)(C5H7O2)] |
M r | 527.28 |
Crystal system, space group | Monoclinic, C2/c |
Temperature (K) | 200 |
a, b, c () | 17.557(2), 17.876(2), 19.832(2) |
() | 91.397(1) |
V (3) | 6222.4(13) |
Z | 16 |
Radiation type | Mo K |
(mm1) | 11.59 |
Crystal size (mm) | 0.18 0.06 0.02 |
Data collection | |
Diffractometer | Bruker APEXII CCD area detector |
Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
T min, T max | 0.48, 0.80 |
No. of measured, independent and observed [I > 2(I)] reflections | 35025, 7103, 6001 |
R int | 0.038 |
(sin /)max (1) | 0.649 |
Refinement | |
R[F 2 > 2(F 2)], wR(F 2), S | 0.027, 0.070, 1.01 |
No. of reflections | 7103 |
No. of parameters | 383 |
H-atom treatment | H-atom parameters constrained |
max, min (e 3) | 3.66, 1.20 |