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. 2015 Sep 30;71(Pt 10):1259–1261. doi: 10.1107/S2056989015017478

Table 3. Experimental details.

Crystal data
Chemical formula [Pt(C11H7BrN)(C5H7O2)]
M r 527.28
Crystal system, space group Monoclinic, C2/c
Temperature (K) 200
a, b, c () 17.557(2), 17.876(2), 19.832(2)
() 91.397(1)
V (3) 6222.4(13)
Z 16
Radiation type Mo K
(mm1) 11.59
Crystal size (mm) 0.18 0.06 0.02
 
Data collection
Diffractometer Bruker APEXII CCD area detector
Absorption correction Multi-scan (SADABS; Bruker, 2014)
T min, T max 0.48, 0.80
No. of measured, independent and observed [I > 2(I)] reflections 35025, 7103, 6001
R int 0.038
(sin /)max (1) 0.649
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.027, 0.070, 1.01
No. of reflections 7103
No. of parameters 383
H-atom treatment H-atom parameters constrained
max, min (e 3) 3.66, 1.20

Computer programs: APEX2 and SAINT (Bruker, 2014), SHELXS97 (Sheldrick, 2008), SHELXL2014 (Sheldrick, 2015), ORTEP-3 for Windows (Farrugia, 2012) and Mercury (Macrae et al., 2008).