| Crystal data |
| Chemical formula |
C27H21FN2O4
|
|
M
r
|
456.46 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c () |
9.7270(19), 10.122(2), 13.441(3) |
| , , () |
68.15(3), 73.69(3), 89.73(3) |
|
V (3) |
1171.4(4) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.09 |
| Crystal size (mm) |
0.30 0.20 0.10 |
| |
| Data collection |
| Diffractometer |
Nonius CAD-4 diffractometer |
| Absorption correction |
scan (North et al., 1968 ▸) |
|
T
min, T
max
|
0.973, 0.991 |
| No. of measured, independent and observed [I > 2(I)] reflections |
4587, 4311, 2756 |
|
R
int
|
0.040 |
| (sin /)max (1) |
0.603 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.054, 0.147, 1.00 |
| No. of reflections |
4311 |
| No. of parameters |
307 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.16, 0.18 |
