Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C12H12N2SCH4O |
| M r | 248.34 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 193 |
| a, b, c () | 7.5959(4), 7.0062(4), 24.4986(14) |
| () | 98.4543(7) |
| V (3) | 1289.61(12) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.24 |
| Crystal size (mm) | 0.24 0.20 0.15 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Integration (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.935, 1.000 |
| No. of measured, independent and observed [I > 2(I)] reflections | 10802, 3055, 2579 |
| R int | 0.025 |
| (sin /)max (1) | 0.663 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.032, 0.090, 1.04 |
| No. of reflections | 3055 |
| No. of parameters | 165 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.28, 0.20 |