Bruker Kappa APEXII CCD diffractometer | 4852 independent reflections |
Radiation source: fine-focus sealed tube | 2432 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.120 |
ω and φ scan | θmax = 27.9°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −36→35 |
Tmin = 0.951, Tmax = 0.964 | k = −16→16 |
26597 measured reflections | l = −15→15 |