Table 1. Summary of data collection and refinement statistics.
| Ube2K~Ub | |
|---|---|
| Data collection | |
| Wavelength (Å) | 0.9537 |
| Resolution (Å) | 47–2.1 (2.16–2.1)a |
| Space group | C2 |
| Unit-cell parameters | |
| a, b, c (Å) | 146.3 37.56 61 |
| α, β, γ (o) | 90 90.43 90 |
| Total reflections | 146692 (11885) |
| Unique reflections | 19503 (1552) |
| Completeness (%) | 99.2 (98.3) |
| I/σ(I) | 10.8 (1.5) |
| Rmerge (%) | 16.2 (157.5) |
| CC1/2 | 0.997 (0.617) |
| Redundancy | 7.5 (7.7) |
| Refinement | |
| Rwork (%) | 19.5 |
| Rfree (%) | 23.5 |
| Non-hydrogen atoms | |
| All atoms | 2249 |
| Protein | 2174 |
| Water | 57 |
| Heterogeneous atoms | 18 |
| Average B factors (Å2) | 24.3 |
| Ramachandran plot (%) | |
| Most favored regions | 97.1 |
| Allowed regions | 2.2 |
| Disallowed regions | 0.7 |
aHigh resolution shell is shown in parentheses.