Table 1.
Entry | E/Z ratio of 1b | Yield (%)a | ee (%)b |
1 | 4.3:1 | 66 | 78 |
2 | 5.7:1 | 65 | 76 |
3 | >99:<1 | 68 | 76 |
aIsolated yield. bDetermined by chiral HPLC analysis.
Entry | E/Z ratio of 1b | Yield (%)a | ee (%)b |
1 | 4.3:1 | 66 | 78 |
2 | 5.7:1 | 65 | 76 |
3 | >99:<1 | 68 | 76 |
aIsolated yield. bDetermined by chiral HPLC analysis.