Experimental apparatus for the recrystallization of ampicillin by GAS process: 1 CO2 cylinder, 2 molecular sieve column, 3 cooler, 4 HPLC pump, 5 valve, 6 spiral heat exchanger, 7 precipitation vessel, 8 sinter metal filter, 9 oven, 10 back pressure valve, 11 organic solvent collection vessel