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. 2015 Oct 29;2015(34):7544–7549. doi: 10.1002/ejoc.201501249

scheme 1.

scheme 1

C–O bond formation with HBF4 at room temperature.[a] dr = diastereoisomeric ratio. [a] Isolated yields; 1H NMR conversions are provided in parentheses when lower than 95 %. [b] 51 % 1H NMR conversion into dimer 3a.