scheme 1.
Synthesis of [4AuCl] and [5AuCl]. Reagents and Conditions: i) [Cu(MeCN)4]PF6, iPr2EtN, EtOH, 80 °C, 18 h; ii) Cl3SiH, Et3N, PhMe/CH2Cl2 (6:1), 100 °C, 18 h; iii) Me2SAuCl, CH2Cl2, RT, 1 h.
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