Table 1.
Spectroscopic properties for the 1H NMR resonance (δ) and IR stretching frequency (υ) of the S–H bond for AdSSH, BnSSH, and TrtSSH compared with their parent thiols.
| δ (ppm) | υSH (cm−1) | |||
|---|---|---|---|---|
| R | RSSH | RSH | RSSH | RSH |
| Trt | 2.75 | 3.10 | 2508 | 2574 |
| Bn | 3.02 | 1.86 | 2504 | 2560 |
| Ad | 2.70 | 1.57 | 2491 | 2567 |