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DoE from 3,6-dihydro-2H-pyran-3-yl diethyl phosphate (2d). Conditions: 4-phenyl-1-butene (2.5 equiv), Cp2ZrHCl (2.0 equiv), 2d (1.0 equiv), CuL* as specified (0.1 equiv), additive as specified (1.0 equiv or 5.0 equiv), in specified solvent (2.0 mL), room temperature. ee determined by HPLC. For more information on the procedures see Supporting Information File 1. ● (wave 1, entries 1–17), ♦ (wave 2, entries 18–30), ▼ (wave 3, entries 31–38).
