Table 3. Synthesis of O,O-Acetals.
| peroxide | acetal | yield (%) |
|---|---|---|
| C8H17OOtBu (11a) | 21a: R = octyl | 57 |
| Ph(CH2)3OOtBu (9a) | 21b: R = (CH2)3Ph | 55 |
| C10H21OOTHP (12b) | 21c: R = decyl | 55 |
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