Table 1.
EXTRACTION MEDIUM | ELUENT | RECOVERIES (%) | |
---|---|---|---|
MELAMINE | CYROMAZINE | ||
Standard solutions | |||
Strata-X (SPE) | 1 mL MeOH 1 mL ACN |
47.5 | 58.7 |
Lichrolut RP-18 (SPE) | 1 mL MeOH 1 mL ACN |
<5% | |
Egg yolk | |||
Strata-X (MSPD) | 1 mL MeOH 1 mL ACN |
34.1 | 12.9 |
QuEChERS | 2 mL ACN | 8.7 | 52.7 |
QuEChERS | 2 mL MeOH | 67.8 | 40.8 |
QuEChERS | 1 mL MeOH 1 mL ACN |
74.5 | 75.3 |