Table 1.

NMR data of fatty acids moieties

	C Shift [ppm]	H Shift [ppm]	Multiplicity	Coupling [Hz]
3′ OH C12:1 FA
O=C1–OH	175.95
–C2H2–	42.39	2.46, 2.24	dd, dd	15.4, 8.25, 4.6
–C3H–OH	69.6	4.00	m
–C4H2–	35.8	2.26	m
–C5H=	125.7	5.43	m
–C6H=	133.5	5.50	m
–C7H2–	28.3	2.05	q	7.1
–C8H2–	30.7	1.37	m
–C9H2–	30.1	1.34	m
–C10H2–	32.9	1.31	m
–C11H2–	23.7	1.33	m
–C12H3	14.4	0.90	t	6.8
C14/C14:1 FA
O=C1–OH	177.8
–C2H2–	35.1	2.27	t	7.4
–C3H2–	26.1	1.59	m
–C4H2–	30.26	1.33
–C5H2–	30.6	1.33
–C6H2–	30.3	1.33
–C7H2–	31.1	1.33	m
–C8H2–	28.17	2.03	dd	12.3, 6.4
–C9H2–/–C9H=	130.9	5.34
–C10H2–/–C10H=	130.9	5.34
–C11H2–	28.17	2.03	dd	12.3, 6.4
–C12H2–	33.1	1.29	m
–C13H2–	23.8	1.32	m
–C14H3	14.6	0.89	t	6.6

Chemical shifts of carbon and hydrogen nuclei, multiplicity of the peak observed and its coupling constant of 3′ hydroxy lauroleic acid from fractions 60–61 (3′OH C12:1 FA) and potential myristic/myristoleic acid from farctions 67–69 (C14/C14:1 FA)

FA fatty acid, d doublet, t triplet, q quartett, m multiplet