Table I.
Data collection and refinement statistics for liganded Fv M6P-1
| Fv M6P-1 with Man6P | |
|---|---|
| Resolution (Å) | 30.1–2.72(2.79–2.72)a |
| Space group | P212121 |
| a (Å) | 60.6 |
| b (Å) | 128.1 |
| c (Å) | 127.3 |
| No. of molecules per asymmetric unit | 4 |
| Rsymb | 0.105 (0.392) |
| I/σ(I) | 7.6 (2.4) |
| Completeness (%) | 81.2 (86.3) |
| Redundancy | 2.5 (2.5) |
| Unique reflections | 20805 |
| Refinement | |
| Rwork (%) | 22.6 |
| Rfree (%) | 26.7 |
| No. of waters | 153 |
| r.m.s bonds (Å) | 0.0090 |
| r.m.s. angles (°) | 1.489 |
| Mean B (Å2) | 30.4 |
| Wilson B (Å2) | 33.0 |
| Ramachandran | |
| Favored | 94% |
| Allowed | 5% |
| Outliers | 1% |
aValues in parentheses represent the highest resolution shell.
bRsym = ΣhklΣi|Ii(hkl) − 〈I(hkl)〉|/ΣhklΣiIi(hkl), where Ii(hkl) is the intensity of each ith redundant observation of reflection hkl, and 〈I(hkl)〉 is the average intensity of a given reflection hkl.