Table 4.
Within-laboratory precision, expressed as relative standard deviation for different working days (RSD), for four different matrices fortified with GlcNAc and GalNAc at the same concentration as was originally detected (n = 5 independent replicates, obtained on three different days by different analysts).
| Recovery (%) | ||||||||
|---|---|---|---|---|---|---|---|---|
| Operator | Raw milk | UHT milk | Yogurt | Infant formula | ||||
| Recovery | RSDc | Recovery | RSDc | Recovery | RSDc | Recovery | RSDc | |
| GlcNAc | ||||||||
| Aa | 101.7 | 0.5 | 101.7 | 0.7 | 102.1 | 0.8 | 97.7 | 1.1 |
| Ba | 101.8 | 1.0 | 101.6 | 0.1 | 98.6 | 1.2 | 100.9 | 0.5 |
| Ca | 102.4 | 0.6 | 103.8 | 0.5 | 100.0 | 1.0 | 102.0 | 1.0 |
|
| ||||||||
| GalNAc | ||||||||
| Ab | 102.5 | 12 | 98.5 | 0.2 | 101.6 | 1.2 | 101.8 | 2.3 |
| Bb | 101.8 | 0.1 | 101.2 | 0.7 | 101.0 | 0.5 | 100.0 | 0.5 |
| Cb | 98.4 | 1.3 | 99.4 | 1.3 | 101.2 | 0.4 | 101.3 | 0.5 |
aThe analyses were performed for determination of GlcNAc by three different operators using four different matrix samples in different days.
bThe analyses were performed for determination of GalNAc by three different operators using four different matrix samples in different days.
cRelative standard deviation (%).