Table 2. Crystallographic data.
| LDH:oxamate | |
|---|---|
| data collection | |
| resolution (Å) | 2.29 |
| space group | P212121 |
| unit cell (Å) | |
| a | 84.1 |
| b | 146.6 |
| c | 284.9 |
| unique reflections a | 158361 (11483) |
| completeness (%) a | 100 (99) |
| Rmerge (%)a | 12.7 (70.2) |
| I/σa | 11.9 (2.7) |
| refinement | |
| R (%) | 17.0 |
| R free (%) | 20.3 |
| all atoms used in refinement | 21652 |
| water | 1321 |
| Validation b (% of all residues) | |
| favoured | 98.0 |
| allowed | 100.0 |
| disallowed | 0.0 |
aValues in parentheses refer to the highest-resolution shell.
bValidation was performed using MolProbity. PDB ID 5ES3