Table 4.
Conditions of eq 2 using i-Pr2NEt•HBF4; [3a] = 0.15 M.
Isolated yield after silica gel chromatography.
Yield measured by 1H NMR relative to an internal standard (1,4-dimethoxybenzene);
ND = not detected.
Conditions of eq 2 using i-Pr2NEt•HBF4; [3a] = 0.15 M.
Isolated yield after silica gel chromatography.
Yield measured by 1H NMR relative to an internal standard (1,4-dimethoxybenzene);
ND = not detected.