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. Author manuscript; available in PMC: 2016 Jun 19.
Published in final edited form as: J Org Chem. 2015 Jun 1;80(12):6025–6036. doi: 10.1021/acs.joc.5b00795

Table 5.

Visible-Light Photocatalytic Coupling of Various Tertiary (N-Acyloxy)phthalimides with (α-Bromomethyl)styrene (14).a

graphic file with name nihms746871t5a.jpg
graphic file with name nihms746871t5b.jpg
a

(N-acyloxy)phthalimide (1 equiv), Ru(bpy)3(PF6)2 (1 mol%), 14 (1.5 equiv), Hantzsch ester 8 (1.5 equiv), i-Pr2NEt (2.2 equiv), blue LEDs, 0.15 M in CH2Cl2, rt, 18 h.

b

Isolated yield after silica gel chromatography (average of two experiments).