Table 3.

¹³C (100 MHz) NMR Spectroscopic Data for Compounds 1-7 (δ in ppm)

	1a	2b	3b	4a	5a	6a	7b
position	δC, type	δC, type	δC, type	δC, type	δC, type	δC, type	δC, type
1	30.9, CH2	29.7, CH2	40.3, CH2	37.9, CH2	31.0, CH2	31.4, CH2	30.4, CH2
2	28.4, CH2	26.2, CH2	103.9, C	108.0, C	29.4, CH2	29.5, CH2	27.1, CH2
3	98.2, C	96.9, C	81.3, CH	75.3, CH	97.8, C	97.3, C	96.7, C
4	50.9, C	49.1, C	44.2, C	48.8, C	53.3, C	52.3, C	51.5, C
5	52.1, CH	51.4, CH	54.5, CH	52.8, CH	45.5, CH	47.0, CH	45.7, CH
6	75.9, CH	75.0, CH	74.7, CH	76.4, CH	75.8, CH	75.1, CH	74.8, CH
7	26.9, CH2	25.7, CH2	24.7, CH2	25.7, CH2	28.0, CH2	35.4, CH2	19.4, CH2
8	118.2, C	109.6, C	109.2, C	110.7, C	28.8, CH	69.2, C	32.8, CH
9	135.0, C	134.3, C	133.8, C	136.5, C	39.4, CH	47.6, CH	37.2, CH
10	36.2, C	35.5, C	48.0, C	48.8, C	33.5, C	34.6, C	33.1, C
11	120.4, CH	100.1, CH	98.7, CH	99.9, CH	35.2, CH2	38.8, CH2	20.9, CH2
12	120.4, CH	152.3, C	152.5, C	153.8, C	195.2, C	194.9, C	26.4, CH2
13	127.9, C	116.7, C	117.0, C	117.9, C	120.9, C	121.0, C	167.1, C
14	154.4, C	154.2, C	154.1, C	155.6, C	172.5, C	169.9, C	82.4, CH
15	107.7, CH	104.3, CH	104.4, CH	105.2, CH	107.1, CH	106.9, CH	114.6, CH
16	146.8, CH	144.0, CH	143.9, CH	145.2, CH	145.3, CH	146.1, CH	173.0, C
18	20.0, CH3	20.0, CH3	22.7, CH3	20.9, CH3	17.4, CH3	18.2, CH3	17.6, CH3
19	181.7, C	180.6, C	180.1, C	181.9, C	180.8, C	180.8, C	179.6, C
20	72.6, CH2	71.2, CH2	72.2, CH2	72.2, CH2	73.9, CH2	75.3, CH2	73.0, CH2
OCH3	-	55.7, CH3	55.7, CH3	56.2, CH3	-	-	-

^aData measured in methanol-d₄.

^bData measured in CDCl₃.