Table 1. X-ray Data collection and refinement statistics.
| Crystal Name | JCV OBD F258L |
|---|---|
| PDB ID | 5CYN |
| Data collection | |
| Wavelength (Å) | 1.075 |
| Space group | I 41 |
| Cell dimensions | |
| A, B, C (Å) | 103.54, 103.54, 34.34 |
| α, β, γ (°) | 90.00, 90.00, 90.00 |
| Resolution (Å) | 50.00–2.7 (2.8–2.7) * |
| R sym or R merge | 0.12 (0.66) |
| I / σI | 37.4 (2.7) |
| Completeness (%) | 99.6 (96.6) |
| Redundancy | 15.4 (7.1) |
| Refinement | |
| Resolution (Å) | 50–2.7 |
| No. reflections | 5163 |
| R work / R free | 19.5, 22.7 |
| No. atoms | 1043 |
| Protein | 1032 |
| Ligand/ion | 4 |
| Water | 7 |
| B-factors | 71.0 |
| Protein | 71.3 |
| Ligand/ion | 61.8 |
| Water | 53.0 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.009 |
| Bond angles (°) | 1.190 |
*Values in parentheses are for highest-resolution shell.