Table 1. Experimental details.
| Crystal data | |
| Chemical formula | [Pt2F(SbF6)2(C8H12)2]SbF6·0.75HF |
| M r | 1347.77 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 133 |
| a, b, c (Å) | 11.325 (4), 15.101 (6), 18.273 (7) |
| β (°) | 100.61 (3) |
| V (Å3) | 3071.7 (19) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 11.81 |
| Crystal size (mm) | 0.10 × 0.10 × 0.02 |
| Data collection | |
| Diffractometer | Bruker SMART CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2006 ▸) |
| T min, T max | 0.721, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 47396, 9265, 7778 |
| R int | 0.041 |
| (sin θ/λ)max (Å−1) | 0.716 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.074, 1.10 |
| No. of reflections | 9265 |
| No. of parameters | 373 |
| H-atom treatment | H-atom parameters constrained |
| w = 1/[σ2(F o 2) + (0.0136P)2 + 38.0407P] where P = (F o 2 + 2F c 2)/3 | |
| Δρmax, Δρmin (e Å−3) | 1.96, −1.66 |