| Rigaku Saturn724+ (2x2 bin mode) diffractometer | 3177 independent reflections |
| Radiation source: Sealed Tube | 2725 reflections with I > 2σ(I) |
| Graphite Monochromator monochromator | Rint = 0.035 |
| Detector resolution: 28.5714 pixels mm-1 | θmax = 27.5°, θmin = 2.3° |
| profile data from ω–scans | h = −4→4 |
| Absorption correction: multi-scan CrystalClear-SM Expert (Rigaku, 20112) | k = −26→26 |
| Tmin = 0.954, Tmax = 0.999 | l = −22→22 |
| 16479 measured reflections |