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. 2016 Jan 1;72(Pt 1):8–13. doi: 10.1107/S2056989015022781
Rigaku Saturn724+ (2x2 bin mode) diffractometer 3177 independent reflections
Radiation source: Sealed Tube 2725 reflections with I > 2σ(I)
Graphite Monochromator monochromator Rint = 0.035
Detector resolution: 28.5714 pixels mm-1 θmax = 27.5°, θmin = 2.3°
profile data from ω–scans h = −4→4
Absorption correction: multi-scan CrystalClear-SM Expert (Rigaku, 20112) k = −26→26
Tmin = 0.954, Tmax = 0.999 l = −22→22
16479 measured reflections