Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C16H14O |
| M r | 222.27 |
| Crystal system, space group | Orthorhombic, P n a21 |
| Temperature (K) | 100 |
| a, b, c (Å) | 13.8369 (9), 12.2202 (8), 6.8468 (4) |
| V (Å3) | 1157.72 (13) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.16 × 0.05 × 0.04 |
| Data collection | |
| Diffractometer | Bruker D8 QUEST area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
| T min, T max | 0.94, 1.00 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 5983, 2024, 1808 |
| R int | 0.038 |
| (sin θ/λ)max (Å−1) | 0.601 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.081, 1.09 |
| No. of reflections | 2024 |
| No. of parameters | 154 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.16, −0.24 |