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. Author manuscript; available in PMC: 2016 Dec 1.
Published in final edited form as: J Colloid Interface Sci. 2015 Aug 5;459:264–272. doi: 10.1016/j.jcis.2015.07.073

Table 2.

Results of HT applied to the sample synthesized using the optimum coprecipitation condition (i.e., stirring rate of 2250 rpm, [Zn+Al] of 20 mM, 2[CO32−]/[Al] of 0.3, and addition rate of 0.416 ml/s)

3 h 5 h 8 h
70 °C χ2 =35.5
NICOMP:
50 nm (15.6%)
322.5 nm (84.4%)
χ2 = 2.34
Gaussian:
327.4 nm
χ2 = 1.68
Gaussian:
309 nm
85 °C χ2 =33.31
NICOMP:
114.1 nm (8.06%)
341.6 nm (91.64%)
χ2 = 0.90
Gaussian:
303.4 nm
χ2 = 1.32
Gaussian:
323 nm