TABLE I.
X-ray plate | Crystallography chip | |
---|---|---|
Crystal parameters | ||
Dominant size in sample (μm) | 40–50 | 40–50 |
Feature width on chip (μm) | NA | 50 |
Data collection | ||
Rotation range: total, increment | 1 deg, 0.1 deg | 1 deg, 0.1 deg |
Exposure time (seconds per image) | 0.5 | 0.5 |
Number of images | 10 | 10 |
Detector distance (mm) | 399.28 | 271.31 |
Wavelength (Å) | 0.9687 | 0.9687 |
Resolution, low (Å) | 21.48 | 16.10 |
Resolution, high (Å) | 1.51 | 1.55 |
Number of reflections | 1779 | 2661 |
Number of reflections, unique | 1741 | 2570 |
Completeness (%) | 4.3 | 6.8 |
Multiplicity | 1.022 | 1.035 |
Rmeas | 0.144 | 0.043 |
⟨I/σ(I)⟩ | 25.0 | 22.20 |
Merging space group | P 4 2 2 | P 4 2 2 |
Unit cell parameters: a = b, c (Å) | 58.39, 151.09 | 58.37, 151.11 |