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. Author manuscript; available in PMC: 2016 Jan 14.
Published in final edited form as: Environ Toxicol Chem. 2012 Jan;31(1):93–99. doi: 10.1002/etc.708

Table 1.

Characterization of bulk and nanoparticulate ZnO by scanning electron microscopy, dynamic light scattering, and zeta potential measurementsa

Manufacturer's reported size (nm) Morphology SEMb Size by DLSc (nm), n = 3 Surface charge by zeta at pH ~8 (mV), n = 2
Bulk - Irregular 1920±151 −14.8±1.2
Alfa Aesar
44904
70 Irregular
Angular
274±8 −18.5±1.2
Alfa Aesar
45409
40 Rounded 159±4 −21.6±3.7
Alfa Aesar
45588
70 Angular 179±3 −23.4±3.1
Consortium 25 Spheroid 215±15 −29.2±1.0
a

The Alfa Aesar nanoparticles (NPs) were observed to have highly polydisperse size distributions by SEM and are, on average, the primary particle size reported by the manufacturer. Error in DLS and zeta potential values is the standard deviation of the mean values reported by the instrument. Additional analysis of all five particles by X-ray diffraction confirmed materials as ZnO (Zincite).

b

SEM = Scanning electron microscopy.

c

DLS = Dynamic light scattering.