| Crystal data |
| Chemical formula |
C15H20O6
|
|
M
r
|
296.31 |
| Crystal system, space group |
Orthorhombic, P212121
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.1980 (1), 10.0290 (2), 16.7720 (3) |
|
V (Å3) |
1378.96 (4) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.92 |
| Crystal size (mm) |
0.65 × 0.47 × 0.30 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur Ruby Gemini |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2013 ▸) |
|
T
min, T
max
|
0.773, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
12778, 2623, 2502 |
|
R
int
|
0.040 |
| (sin θ/λ)max (Å−1) |
0.613 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.035, 0.096, 1.05 |
| No. of reflections |
2623 |
| No. of parameters |
200 |
| Δρmax, Δρmin (e Å−3) |
0.27, −0.17 |
| Absolute structure |
Flack (1983 ▸), 1073 Friedel pairs |
| Absolute structure parameter |
−0.09 (9) |
