Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Fe(PO4)(N2H4)] |
| M r | 182.87 |
| Crystal system, space group | Orthorhombic, P c c n |
| Temperature (K) | 293 |
| a, b, c (Å) | 6.3114 (13), 7.6680 (15), 8.6485 (18) |
| V (Å3) | 418.55 (15) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 3.89 |
| Crystal size (mm) | 0.05 × 0.03 × 0.03 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.668, 0.746 |
| No. of measured, independent and observed [I > 3σ(I)] reflections | 13820, 601, 457 |
| R int | 0.065 |
| (sin θ/λ)max (Å−1) | 0.717 |
| Refinement | |
| R[F 2 > 3σ(F 2)], wR(F 2), S | 0.020, 0.027, 1.46 |
| No. of reflections | 601 |
| No. of parameters | 47 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.40, −0.33 |