| Bruker APEXII DUO CCD area-detector diffractometer | 12002 independent reflections |
| Radiation source: fine-focus sealed tube | 7987 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.048 |
| φ and ω scans | θmax = 30.2°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −13→14 |
| Tmin = 0.730, Tmax = 0.830 | k = −16→16 |
| 78666 measured reflections | l = −26→26 |