| Bruker SMART APEX CCD diffractometer | 10033 independent reflections |
| Radiation source: fine-focus sealed tube | 6949 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.050 |
| Detector resolution: 8.3333 pixels mm-1 | θmax = 29.6°, θmin = 1.6° |
| φ and ω scans | h = −14→15 |
| Absorption correction: multi-scan (SADABS; Bruker, 2015) | k = −20→20 |
| Tmin = 0.86, Tmax = 0.99 | l = −31→31 |
| 70656 measured reflections |