Bruker SMART APEXII CCD area-detector diffractometer | 7990 independent reflections |
Radiation source: sealed tube | 6137 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.043 |
Detector resolution: 8 pixels mm-1 | θmax = 32.6°, θmin = 1.9° |
ω and φ scans | h = −19→20 |
Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −22→22 |
Tmin = 0.720, Tmax = 0.862 | l = −33→34 |
32242 measured reflections |