Table 6.
Topas full Rietveld model parameters
| Parameter | Value | Parameter | Value |
|---|---|---|---|
| Zero Error | −0.0268° | Displacement | −0.016 mm |
| Rp, Rs | 217.5 mm | Rec. slit width | 75 µm |
| Fil. Length | 8 mm | Samp. Length | 15 mm |
| Rec. slit length | 12 | Sample Absorption | 126.8 cm−1 |
| CSL | 3027 nm | CSG | 488 nm |
| Lattice spacing | 4.156925692 Å | Equat. Diverg. | 1.096° |
| Source Spectrum | |||
| intensity (la) | wavelength (Å) (lo) | Lor. width (mÅ) (lh) | Gauss. width (mÅ) (lg) |
| 1 | 1.540591 | 0 | 0.4323 |
| 0.7504 | 1.540591 | 0 | 1.6718 |
| 0.0418 | 1.540591 | 0 | 3.9651 |
| 0.1861 | 1.541064 | 0 | 0.4565 |