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An extended solvent screening for the base metal-catalyzed aerobic oxidation reaction.a
 | |||
| Entry | Solventb | Yield 16 (%)c | Yield 17 (%)c |
| 1 | DMSOd | 0 | 87 |
| 2 | anisolee | 0 | 85 |
| 3 | n-BuOAce | 0 | 89 |
| 4 | 1,4-dioxanef | 2 | 85 |
| 5 | toluened | 18 | 67 |
| 6 | CPMEd | 5 | 80 |
| 7 | n-BuOHe | 5 | 73 |
aReactions were performed on a 5 mmol scale in 10 mL of solvent using 1 atmosphere of O2 (balloon). bClassification of solvents as provided in [44]. cIsolated yields. dProblematic. eRecommended. fHazardous.
