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. 2016 Jan 21;7:10401. doi: 10.1038/ncomms10401

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(a) HSQC spectrum of Au₁₀₂(pMBA)₄₄ cluster in 0.3 M D₂O–NaOH showing assignment of ¹H–¹³C correlation peaks. For some of the less-mobile ligands, correlation peaks for both a₁ and a₂ and/or b₁ and b₂ carbons could be identified. Inset shows the entire spectrum with higher signal-to-noise level and ND denotes ‘not determined'. (b,c) Calculated ¹H–¹³C correlation chemical shifts. (c) The congested area in b in a larger scale.