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Mass spectrometry data for psBBOX‐catalyzed hydroxylations: a) natural substrate γ‐BB 1; b) phosphorus analogue 2; c) arsenic analogue 3; d) neutral carbon analogue 4. Top panel=starting substrate; bottom panel=psBBOX‐catalyzed reaction [a–c) 1 μm psBBOX, 5 min; d) 10 μm psBBOX, 3 h].
