Table 1. Data-collection statistics.
Values in parentheses are for the highest resolution shell. N/D, not determined.
Protein | Cas5a | LptA | ||
---|---|---|---|---|
Conditions | Dehydrated, cryoprotected | Cryoprotected | Room temperature | Dehydrated, cryoprotected |
Space group | P21 | P21 | P21 | P3221 |
Unit-cell parameters | ||||
a (Å) | 75.92 | 76.70 | 76.01 | 146.98 |
b (Å) | 42.54 | 44.47 | 43.81 | 146.98 |
c (Å) | 89.64 | 91.39 | 90.11 | 193.12 |
α (°) | 90 | 90 | 90 | 90 |
β (°) | 111.85 | 110.34 | 112.04 | 90 |
γ (°) | 90 | 90 | 90 | 120 |
Resolution (Å) | 50–1.94 (1.97–1.94) | <3.5 | <4 | 50–3.40 (3.46–3.40) |
Unique reflections | 39309 | N/D | N/D | 63515 |
Completeness (%) | 99.4 (92.6) | N/D | N/D | 99.5 (99.5) |
Multiplicity | 3.8 (2.3) | N/D | N/D | 4.5 (4.4) |
〈I/σ(I)〉 | 12.82 (1.17) | N/D | N/D | 12.30 (2.61) |
R merge | 0.11 (0.60) | N/D | N/D | 0.17 (0.54) |
Solvent content (%) | 42.8 | 47.4 | 44.7 | 52.9 |