. 2016 Feb 5;6:20575. doi: 10.1038/srep20575

Table 1. Data collection and refinement statistics for glucosidase II α catalytic subunit.

	Tris-bound		SeMet Apo		DNJ-bound
Crystallographic data
Space group	R32		R32		R32
Unit cell a/b/c (Å)	189.0/189.0/157.2		189.3/189.3/158.0		189.5/189.5/157.8
Data processing statistics
Beam line	PF BL5A		PF-AR NE3A		PF-AR NE3A
Wavelength (Å)	1.00000		0.97946		0.97946
Resolution (Å)	50–1.40 (1.42–1.40)		50–2.40 (2.44–2.40)		50–1.60 (1.63–1.60)
Total/unique reflections	1,537,957/209,648		470,213/42,596		766,615/141,836
Completeness (%)	99.9 (100.0)		100.0 (100.0)		98.3 (98.0)
R_merge (%)	6.0 (41.0)		12.3 (45.5)		8.6 (41.9)
I/σ (I)	46.3 (5.9)		26.7 (6.4)		23.6 (2.8)
Refinement statistics
Resolution (Å)	20.0–1.40				20.0–1.60
R_work/R_free (%)	15.4/17.5				15.5/18.3
R.m.s. deviations from ideal
Bond lengths (Å)	0.010				0.011
Bond angles (°)	1.40				1.43
Ramachandran plot (%)
Most Favored	87.8				87.8
Additionally allowed	11.9				11.9
Generously allowed	0.3				0.3
Disallowed	0				0

		α3-Glc₂-bound		Man₂Glc₁-bound
Crystallographic data
Space group		R32		R32
Unit cell a/b/c (Å)		190.0/190.0/158.6		189.7/189.7/158.3
Data processing statistics
Beam line		SPring-8 BL44XU		SPring-8 BL44XU
Wavelength (Å)		0.90000		0.90000
Resolution (Å)		50–2.40 (2.44–2.40)		50–2.30 (2.34–2.30)
Total/unique reflections		323,577/43,022		365,028/48,696
Completeness (%)		100.0 (100.0)		100.0 (100.0)
R_merge (%)		9.3 (43.3)		10.8 (45.7)
I/σ (I)		33.5 (6.4)		31.6 (7.2)
Refinement statistics
Resolution (Å)		20.0–2.40		20.0–2.30
R_work/R_free (%)		14.8/19.9		14.4/18.9
R.m.s. deviations from ideal
Bond lengths (Å)		0.010		0.012
Bond angles (°)		1.34		1.45
Ramachandran plot (%)
Most Favored		85.4		86.4
Additionally allowed		14.2		13.2
Generously allowed		0.4		0.4
Disallowed		0		0