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. 2013 May 21;2013:719593. doi: 10.1155/2013/719593

Table 2.

Extraction yields and radical scavenging percentages of several extracts prepared by the extraction procedures E1–E6 from the olive wood sample A.

Extracta Procedureb Solvent Temperature Yieldc RSP ± SDd
A1 E1 EtOH r.t. 54.1 48.8 ± 0.2

A2 E2 EtOAc r.t. 11.0 63.2 ± 0.8
A3 E2 EtOH r.t. 51.4 42.1 ± 0.4

A4 E3 EtOAc Reflux 14.2 64.9 ± 0.1

A5 E4 EtOAc r.t. 8.6 48.5 ± 0.8
A6 E4 EtOH r.t. 40.0 42.1 ± 1.1
A7 E4 EtOH : H2O 3 : 2 r.t. 111.4 27.1 ± 1.9
A8 E4 H2O r.t. 80.0 17.1 ± 1.4
A9 E4 H2O : HCOOH 4 : 1 r.t. 122.9 25.9 ± 0.5
A10 E4 EtOAc Reflux 11.4 50.9 ± 1.5
A11 E4 EtOH Reflux 94.3 52.4 ± 1.7
A12 E4 EtOH : H2O 3 : 2 Reflux 145.7 39.6 ± 1.1
A13 E4 H2O Reflux 108.6 44.0 ± 0.2
A14 E4 H2O : HCOOH 4 : 1 Reflux 211.4 33.7 ± 1.8

A15 E5 EtOAc Reflux 22.6 54.3 ± 0.3
A16 E5 n-BuOH Reflux 54.9 45.7 ± 1.3
A17 E5 H2O Reflux 42.0 11.1 ± 0.8

A18 E6 Et2O Reflux 4.0 48.5 ± 0.1
A19 E6 CHCl3 Reflux 4.0 26.1 ± 0.4
A20 E6 n-BuOH Reflux 33.7 39.6 ± 0.1

Rosemary oleoresin (reference extract)d 95.0 ± 0.3

aExtracts A1–A20 were prepared from the olive wood sample A, collected in April, 2003 (during the pruning period) at the village of Fuensanta, Jaén province, Spain.

bProcedures E1–E6 are detailed in Figures 16.

cYield is expressed as grams of extract per kilogram of olive wood sample.

dRadical scavenging percentage (RSP) is expressed as DPPH scavenging (%). Values are means of three replicates ± SD (standard deviation).

dCommercially available rosemary extract was used as reference, at the same concentration (50 μg mL−1).