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a (a) EDCI, HOBt, NMM, CH3OCH3NH·HCl, CH2Cl2, 51–95%; (b) 3,4,5-trimethoxyphenyl-magnesium bromide, THF, 48–78%; (c) LAH, −78 °C, THF, 85%; (d) Dess–Martin reagent, CH2Cl2, 81%; (e) EDCI, HOBt, NMM, 3,4,5-trimethoxybenzoic acid, CH2Cl2, 58%.
