Table 1.
Crystallographic data collection and refinement statistics
| Nup98•Nb TP377 complexa |
|
|---|---|
| Data collection | |
| Space group | P41 |
| Cell dimensions | |
| a, b, c (Å) | 66.59, 66.59, 87.90 |
| α, β, γ (°) | 90.00, 90.00, 90.00 |
| Resolution (Å) | 47.00-1.90 (1.95-1.90)b |
| Rsym or Rmerge | 0.128 (>1)b |
| I / σI | 27.7 (2.6)b |
| Completeness (%) | 99.5 (98.7)b |
| Redundancy | 27.4 (27.4)b |
| Refinement | |
| Resolution (Å) | 47.00-1.90 |
| No. reflections | |
| Measured | 823105 |
| Unique | 30218 |
| Rwork/Rfree | 0.167 / 0.196 |
| No. atoms | |
| Protein | 2176 |
| Water | 145 |
| Wilson B-factor (Å2) | 27.4 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.010 |
| Bond angles (°) | 1.08 |
| Ramachandran statistics (%) | |
| Favored | 98.0 |
| Allowed | 2.0 |
| Outliers | - |
aA single crystal was used for data collection.
bValues in parentheses are for highest resolution shell.