| Space group |
P1 |
| Cell dimensions, Å |
a = 69.0, b = 77.2, c = 86.2 |
|
α = 63.9, β = 75.0, γ = 89.39 |
| Data collection |
| Resolution limit, Å |
2.3 |
| Unique reflections |
58 583 |
| Completeness (overall/last shell),% |
86.2/89.1 |
| Rsym (overall/last shell),% |
10.3/31.2 |
| I/ σI (overall/last shell) |
13.3/11.7 |
| Redundancy (overall/last shell) |
2.3/2.0 |
| Refinement |
| Average B-factor, Å2
|
| macromolecule (protein, RNA) |
29.1 |
| solvent (water, ions) |
32.7 |
| ligands |
60.2 |
| Number of atoms |
| macromolecule (protein, RNA) |
9944 |
| ligand |
22 |
| solvent molecules (water, ions) |
636 |
| Rwork (|F| > 0σ),% |
16 |
| Rfree (|F| > 0σ),% |
20 |
| Rms deviations from ideality |
| Bond lengths, Å |
0.008 |
| Bond angles, ° |
1.10 |
