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(A) 1D 1H NMR spectra of Fmoc-DOPA assembly by solution NMR at different time points. (B) 2D 1H radio frequency–driven recoupling (RFDR) data of lyophilized Fmoc-DOPA samples prepared immediately (time 0), 2 hours, 5 hours, and 1 month after the assembly was initiated.
