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MS/MS fragmentation patterns recorded at the 20% HCD level from a disulfated and fucosylated bikunin CS-glycopeptide precursor ion. A, The complete HCD spectrum of the [M+3H]3+ precursor ion at m/z 1143.11. B, The complete HCD spectrum of the [M+3Na]3+ precursor ion at m/z 1165.09, and C, the expanded m/z 1000–1500 region of the sodiated precursor ion.
